THIOPHENE-2-ACETAMIDE
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- Molecular Formula: C6H7NOS
- Molecular Weight: 141.194
- Vapor Pressure: 0.000207mmHg at 25°C
- Melting Point: 145oC
- Boiling Point: 327°Cat760mmHg
- Flash Point: 151.6°C
- PSA： 71.33000
- Density: 1.254g/cm3
- LogP: 1.47620
THIOPHENE-2-ACETAMIDE(Cas 4461-29-4) Usage
InChI:InChI=1/C6H7NOS/c7-6(8)4-5-2-1-3-9-5/h1-3H,4H2,(H2,7,8)
4461-29-4 Relevant articles
A CO2-mediated base catalysis approach for the hydration of triple bonds in ionic liquids
Han, Buxing,Ke, Zhengang,Li, Ruipeng,Liu, Zhimin,Tang, Minhao,Wang, Yuepeng,Zeng, Wei,Zhang, Fengtao,Zhao, Yanfei
supporting information, p. 9870 - 9875 (2021/12/27)
Herein, we report a CO2-mediated base ca...
One-pot method for the synthesis of 1-aryl-2-aminoalkanol derivatives from the corresponding amides or nitriles
Bobal, Pavel,Otevrel, Jan,Svestka, David
, p. 25029 - 25045 (2020/07/14)
We have identified a novel one-pot metho...
[18F]MALEIMIDE-BASED GLYCOGEN SYNTHASE KINASE-3BETA LIGANDS FOR POSITRON EMISSION TOMOGRAPHY IMAGING AND RADIOSYNTHESIS METHOD
-
Page/Page column 68, (2018/08/03)
The present invention provides a compoun...
Corresponding amine nitrile and method of manufacturing thereof
-
Paragraph 0138; 0139; 0140; 0151; 0152, (2018/05/07)
The invention relates to a manufacturing...
4461-29-4 Process route
-
-
88-15-3,97511-16-5
2-Acetylthiophene
-
-
4461-29-4
2-(thiophen-2-yl)acetamide
| Conditions | Yield |
|---|---|
|
With
ammonium hydroxide; sulfur;
In
ethanol;
at 120 ℃;
for 8h;
under 600.06 - 15001.5 Torr;
Pressure;
Temperature;
|
99.5%
|
|
With
ammonium hydroxide; ammonium polysulfide; sulfur;
Reagens 4: Dioxan;
|
-
-
1918-77-0
Thiophene-2-acetic acid
-
-
4461-29-4
2-(thiophen-2-yl)acetamide
| Conditions | Yield |
|---|---|
|
Thiophene-2-acetic acid;
With
thionyl chloride;
In
dichloromethane;
at 0 ℃;
for 2h;
With
ammonium hydroxide;
In
tetrahydrofuran;
at 0 - 20 ℃;
|
72%
|
|
Multi-step reaction
with
2
steps
1: toluene-4-sulfonic acid
2: aqueous ammonia
With
ammonium hydroxide; toluene-4-sulfonic acid;
|
|
|
Multi-step reaction
with
2
steps
1: thionyl chloride
2: aqueous ammonia
With
ammonium hydroxide; thionyl chloride;
|
|
|
In
dichloromethane;
|
|
|
With
ammonia; 1,1'-carbonyldiimidazole;
In
tetrahydrofuran; methanol;
|
|
|
Multi-step reaction
with
2
steps
1: thionyl chloride / dichloromethane / 2 h / 0 °C / Reflux
2: ammonium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C
With
ammonium hydroxide; thionyl chloride;
In
tetrahydrofuran; dichloromethane; water;
|
|
|
With
ammonia;
at 125 ℃;
for 0.5h;
Temperature;
|
|
|
Multi-step reaction
with
2
steps
1: thionyl chloride / 0.5 h / 25 °C / Inert atmosphere
2: ammonia / water / 0.5 h / 25 °C
With
thionyl chloride; ammonia;
In
water;
|
4461-29-4 Upstream products
-
1918-82-7
2-vinylthiophene
-
20893-30-5
2-cyanomethylthiophene
-
88-15-3
2-Acetylthiophene
-
39098-97-0
2-thienylacetic acid chloride
4461-29-4 Downstream products
-
20893-30-5
2-cyanomethylthiophene
-
1003-31-2
thiophene-2-carbonitrile
-
30433-91-1
[2-(2-thyenyl)ethyl]amine
-
349426-88-6
N-(2-ethylphenyl)-2-(thiophen-2-yl)acetamide
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